When CubeSat projects are a useful means by which universities can engage their students in space-related activities. TURKSAT-3USAT is a three-unit amateur radio CubeSat jointly developed by the Space Systems Design and Test Laboratory and the Radio Frequency Electronics Laboratory of Istanbul Technical University (ITU), in collaboration with TURKSAT, A.S. company as well as the Turkish Amateur Technology Organization. It was launched on April 26, 2013 as a secondary payload on a CZ-2D rocket from China’s Jiuquan Space Center to an altitude of approximately 680 km. The mission of the satellite has two primary goals: (1) to voice communication at Low Earth Orbit (LEO) and (2) to educate students by providing hands-on experience. TURKSAT-3USAT was designed to sustain a circular, near sun-synchronous LEO, and has dimensions of 10 x 10 x 34 cm3. Within the course of this paper, TURKSAT-3USAT’s thermal control will be addressed. TURKSAT-3USAT’s thermal control model was developed using ThermXL and ESATAN-TMS software. Using this model, temperature distributions of the CubeSat when subjected to various experimental conditions of interest were computed. Using a thermal vacuum chamber (TVAC), thermal cycling and bake-out testing were carried out on the flight model to verify the thermal design performance and check the mathematical model. Based on thermal analysis results, the temperature of equipment was within the allowable temperature range except for the batteries that were between 42.56 oC and -20.31 oC. Heaters were used for the batteries in order to maintain the batteries’ temperature within the allowable temperature range.